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Year 2005, Month 5 (Section Full Articles, Page 1245)

Phosphorus-containing disiloxanes: synthesis and thermal rearrangement of the 1,2-shift type

G. N. Molchanova,* T. M. Shcherbina, P. V. Petrovskii, and E. E. Nifant`ev

Methods for the synthesis of tetramethylbis(ω-phosphoryloxyalkyl)disiloxanes were devel- oped. Thermal rearrangement of the 1,2-shift type of tetramethylbis(phosphoryloxymethyl)di- siloxanes was studied. The 1,2-shift rearrangement of dimethyl(diphenoxyphosphoryloxy- methyl)silyl hydrogen sulfate was found.

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